Fabrication and Properties of Stainless-Steel Foams with Simultaneous Use of Two Different Space Holders

Document Type : Research Paper

Authors

Department of Materials Science and Engineering, School of Engineering, Shiraz University, Shiraz, Iran

Abstract

In this study, low-density yet high-strength 316L stainless steel foam was successfully fabricated using the powder metallurgy technique. This was achieved by employing both carbamide and steel hollow spheres as space holders to tailor porosity and mechanical properties. The volumetric percentage of carbamide was varied from 0 to 50% to investigate its effect on density, while steel hollow spheres (0%–50% by volume) were incorporated to enhance strength. The fabrication process involved layer-by-layer deposition of stainless steel powder and space holders in a mold, followed by uniaxial compaction at 150 MPa using polyvinyl alcohol as a binder. Carbamide was removed through heat treatment at 120–180 °C in ambient conditions, and the samples were subsequently sintered at 1150 °C for 3 hours in a neutral atmosphere. Following optimization of fabrication parameters and porosity control, the samples were characterized using compression tests and scanning electron microscopy (SEM) to evaluate their mechanical performance and microstructural evolution. Compression test results revealed that increasing carbamide content decreased the density, whereas a higher percentage of steel hollow spheres significantly improved compressive strength, reaching a maximum of 528.70 MPa at constant porosity. SEM analysis confirmed that the replacement of carbamide with steel hollow spheres led to the transformation of open-cell porosity into closed-cell porosity.

Keywords


[1]   Banhart, J. (1999). Foam metal: the recipe. Europhysics News, 30(1) 17-20. https://doi.org/10.1007/s00770-999-0017-8
[2]   Pérez, L., Mercado, R., & Alfonso, I. (2017). Young's modulus estimation for CNT reinforced metallic foams obtained using different space holder particles. Composite Structures, 168, 26-32. https://doi.org/10.1016/j.compstruct.2017.02.017
[3]   Mutlu, I., & Oktay, E. (2011). Production and characterization of Cr-Si-Ni-Mo steel foams. Indian Journal of Engineering and Materials Science, 18(3), 227-232. http://nopr.niscpr.res.in/handle/123456789/12470
[4]   Rosip, N. M., Ahmad, S., Jamaludin, K., & Noor, F. M. (2013). Producing of 316l stainless steel (SS 316L) foam via slurry method. Journal of Mechanical Engineering and Sciences, 5, 707-712. https://doi.org/10.15282/jmes.5.2013.17.0068
[5]   Besharati, F., & Paydar, M. H. (2023). Fabrication of copper open cell foam by electrochemical deposition method and investigation on the effect of current intensity and plating solution on the created microstructure. Iranian Journal of Materials Forming, 10(1), 4-12. https://doi.org/10.22099/ijmf.2023.46551.1245
[6]   Hassanli, F., & Paydar, M. H. (2022). Effect of green body formation by single and double action pressing on the mechanical properties of al foams. Iranian Journal of Materials Forming, 9(1) 5-12. https://doi.org/10.22099/ijmf.2022.42018.1197
[7]   Smith, B., Szyniszewski, S., Hajjar, J., Schafer, B., & Arwade, S. (2011). Steel foam for structures: A review of applications, manufacturing and material properties. Journal of Constructional Steel Research, 71, 1-10. https://doi.org/10.1016/j.jcsr.2011.10.028
[8]   Babcsán, N., Banhart, J., & Leitlmeier, D. (2003, November). Metal foams–manufacture and physics of foaming. In Proceedings of the International Conference Advanced Metallic Materials (Vol. 5, p. 15).
[9]   Nakajima, H., Hyun, S. K., Park, J. S., Tane, M. (2007, February). Fabrication of louts-type porous petals by continuous zone pelting and continuous casting techniques. In Materials Science Forum (Vol. 539, pp. 187-192). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/MSF.539-543.187
[10] Rabiei, A., & Vendra, L. (2009). A comparison of composite metal foam's properties and other comparable metal foams. Materials Letters, 63(5), 533-536. https://doi.org/10.1016/j.matlet.2008.11.002
[11] Stanev, L., Kolev, M., Drenchev, B., & Drenchev, L. (2017). Open-cell metallic porous materials obtained through space holders—Part II: structure and properties. a review. Journal of Manufacturing Science and Engineering, 139(5), 050802-050833. https://doi.org/10.1115/1.4034440
[12] Bekoz, N., & Oktay, E. (2012). Effects of carbamide shape and content on processing and properties of steel foams. Journal of Materials Processing Technology, 212(10), 2109-2116. https://doi.org/10.1016/j.jmatprotec.2012.05.015
[13] Mirzaei, M., & Paydar, M. H. (2017). A novel process for manufacturing porous 316 L stainless steel with uniform pore distribution. Materials & Design, 121(5), 442-449. https://doi.org/10.1016/j.matdes.2017.02.069
[14] Besharati, F., & Paydar, M. H. (2024). Investigation on the microstructure and compressive behavior of open-cell copper-Al2O3 composite foams. Journal of Materials Research and Technology, 33, 3427–3438. https://doi.org/10.1016/j.jmrt.2024.10.059
[15] Xia, X. C., Chen, X. W., Zhang, Z., Chen, X., Zhao, W. M., Liao, B. & Hur, B. (2013). Effects of porosity and pore size on the compressive properties of closed-cell Mg alloy foam. Journal of Magnesium and Alloys, 1(4), 330-335. https://doi.org/10.1016/j.jma.2013.11.006
[16] Hassanli, F., & Paydar, M. H. (2021). Improvement in energy absorption properties of aluminum foams by designing pore-density distribution. Journal of Materials Research and Technology, 14, 609–619. https://doi.org/10.1016/j.jmrt.2021.06.073